94,295 datasets found

Sodium bicyclo[1.1.1]pentylsulfinate (154 mg, 1.00 mmol, 1.00 equiv) was dissolved in 2-methyltetrahydrofuran (2.00 mL) under argon. Chloro(trimethyl)silane (163 mg, 190 μL,...

dataset for 1H nuclear magnetic resonance spectroscopy (1H NMR)

Methyl 3-(1-bicyclo[1.1.1]pentanylsulfonyl)propanoate (1.36 g, 6.22 mmol, 1.00 equiv) was dissolved in tetrahydrofuran (14 mL) and stirred at 21 °C. Potassium tert-butoxide in...

dataset for 1H nuclear magnetic resonance spectroscopy (1H NMR)

dataset for 13C nuclear magnetic resonance spectroscopy (13C NMR)

dataset for electrospray ionisation quadrupole detection (ESI Q Trap)

dataset for 1H--13C heteronuclear single quantum coherence (1H-13C HSQC)

dataset for infrared absorption spectroscopy (IR)

In an argon flushed 10 mL flask a methyl 3-sulfanylpropanoate (14.7 g, 13.5 mL, 122 mmol, 1.30 equiv) in diethyl ether (125.00 mL) was added to Tricyclo[1.1.1]pentane (6.22 g,...

dataset for 1H nuclear magnetic resonance spectroscopy (1H NMR)

The methyl 3-(1-bicyclo[1.1.1]pentanylsulfanyl)propanoate (14.0 g, 75.2 mmol, 1.00 equiv) was dissolved in dichloromethane (140 mL) and cooled to 0 °C in an ice bath....

dataset for 1H nuclear magnetic resonance spectroscopy (1H NMR)

The sodium bicyclo[1.1.1]pentylsulfinate (1.00 g, 6.49 mmol, 1.00 equiv) was disolved in H2O (2mL). The solution was acidified by adding 1M HCl (pH = 1) and poured into a...

dataset for 1H nuclear magnetic resonance spectroscopy (1H NMR)

dataset for electrospray ionisation quadrupole detection (ESI Q Trap)

dataset for 1H--13C heteronuclear single quantum coherence (1H-13C HSQC)

dataset for 13C nuclear magnetic resonance spectroscopy (13C NMR)

dataset for infrared absorption spectroscopy (IR)

Sodium bicyclo[1.1.1]pentylsulfinate (77.1 mg, 500 μmol, 1.00 equiv) was dissolved in 2-methyltetrahydrofuran (1.00 mL) under argon. Chloro(trimethyl)silane (81.5 mg, 95.2 μL,...

dataset for 1H nuclear magnetic resonance spectroscopy (1H NMR)