Short-RInChIKey=SA-FUHFF-UHFFFADPSC-IHUUETIJAD-UHFFFADPSC-NUHFF-GUHFF-NUHFF-ZZZ

Every synthesis is carried out on a TX-60 6-axis robot from Stäubli in a glovebox under nitrogen atmosphere. From every synthesis two samples are produced. For the synthesis solutions of copper di-acetate monohydrate in 210 mL ethanol and trimesic acid in ethanol includng the modulator water (total volume 210 mL) are prepared separately via ultrasonication --> See Tab "SURMOF Reaction". During the synthesis, the functionalized substrates are subsequently immersed in different solutions in a fixed sequence --> see Tab "SURMOF Reaction". The concentrations of the starting materials A and B are applied in cycles 1 to 3. Subsequently the solutions are swapped immediately after cycle no 3 and the concentrations of starting materials C and D are applied during cycles 4 to 40. All together the synthesis comprises 40 cycles.