Dataset

Short-RInChIKey=SA-FUHFF-UHFFFADPSC-JGPWTFKOWR-UHFFFADPSC-NUHFF-NQWWQ-NUHFF-ZZZ

3-(3,5-Dimethoxyphenyl)-3-hydroxy-2H-isoindol-1-one (143 mg, 500 μmol, 1.00 equiv) and N-[(E)-prop-1-enyl]benzamide (101 mg, 625 μmol, 1.25 equiv) were disolved in DCM (5 mL) and cooled to 0 °C. p-Toluenesulfonic acid monohydrate (9.51 mg, 50.0 μmol, 0.100 equiv) was added and the reaction stirred for 2 h. The reaction was quenched by addition of saturated aqueous NaHCO3-solution (10mL). The organic layer was separated and the aqueous phase was extracted with dichloromethane (2x 5 mL). The combined organic layers were dried over Na2SO4 and the solvent was evaporated under reduced pressure.

Chemical Info

InChI Short-RInChIKey=SA-FUHFF-CUSBTMCTUJ-JGPWTFKOWR-WNONGYQPIM-NFBDV-NQWWQ-NUHFF-ZZZ

Data and Resources

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Metadata Information

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License URL https://creativecommons.org/licenses/by/4.0
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Author Hałaczkiewicz, Miro, Maraj, Arianit, Kelm, Harald, Manolikakes, Georg
Maintainer chemotion-repository
Language en
MetadataCreated 2024-01-24T11:59:58.115144
MetadataModified 2024-01-24T11:59:58.115150
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