Dataset

Short-RInChIKey=SA-FUHFF-UHFFFADPSC-KYQMJVXFEU-UHFFFADPSC-NUHFF-NUEKX-NUHFF-ZZZ

4-(Methylthio)aniline (732 mg, 5.26 mmol, 1.00 equiv) and 1H-pyrrole-2-carbaldehyde (500 mg, 5.26 mmol, 1.00 equiv) were added to a flask together with 5 g of molecular sieves 4Å and 25 mL of DCM. The reaction mixture was refluxed for 24 hours, then the molecular sieves were filtered off, then the molecular sieves were filtered off, and the solvent was evaporated under reduced pressure. The product was treated with 5 mL of pentane to afford a solid that was filtered off, washed with 2x2.5 mL of pentane and dried in vacuo. The compound (E)-N-(4-(methylthio)phenyl)-1-(1H-pyrrol-2-yl)methanimine (810 mg, 3.56 mmol, 68% yield) was isolated as a brown powder.

Chemical Info

InChI Short-RInChIKey=SA-BUHFF-KYQMJVXFEU-WABFJHIZRR-YMWUJEATGC-NUEKX-NUHFF-NUHFF-ZZZ

Data and Resources

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License URL https://creativecommons.org/licenses/by/4.0
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Author Ferraro, Valentina
Maintainer chemotion-repository
Language en
MetadataCreated 2024-04-20T09:00:08.177230
MetadataModified 2024-04-20T09:00:08.177235
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