Short-RInChIKey=SA-FUHFF-UHFFFADPSC-MRDPMFJFXN-UHFFFADPSC-NUHFF-NUHFF-NUHFF-ZZZ

The propellane solution (28.9 mg, 1.00 mL, 437 μmol, 1.00 equiv) was added to a solution of (phenyldisulfanyl)benzene (143 mg, 655 μmol, 1.50 equiv) and 1-methoxy-4-[(4-methoxyphenyl)disulfanyl]benzene (182 mg, 655 μmol, 1.50 equiv) in THF (1.00 mL) under argon atmosphere and the mixture was irradiated with UV light (500 W) for 20 min. After evaporation of the solvent under reduced pressure, the crude residue was purified via column chromatography and preparative TLC.