Dataset

Short-RInChIKey=SA-FUHFF-UHFFFADPSC-QNBPDVUHGI-UHFFFADPSC-NUHFF-NUHFF-NUHFF-ZZZ

To a solution of methyl 2,2-dimethylchromene-6-carboxylate (56.6 mg, 259 μmol, 1.00 equiv) in 2.7 mL of dry THF was added lithium aluminum hydride (32.5 mg, 856 μL, 856 μmol, 1.00 M in THF, 3.30 equiv) and the mixture was refluxed (64 °C) for 2 h. After cooling down to 21 °C, 1 M NaOH solution was added. The aqueous phase was extracted with diethyl ether twice then the combined organic layers were washed with water and brine. The combined organic layers were dried over sodium sulfate and coated onto Celite.

Chemical Info

InChI Short-RInChIKey=SA-BUHFF-QNBPDVUHGI-BVQOOKUOYK-YEEQAHZWDX-NUHFF-NUHFF-NUHFF-ZZZ

Data and Resources

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Metadata Information

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DOI
License URL https://creativecommons.org/licenses/by-sa/4.0
Source
Version
Author Vanderheiden-Schroen, Sylvia, Volz, Nicole
Maintainer chemotion-repository
Language en
Measurement Technique IRI
MetadataCreated 2024-02-10T09:57:35.878765
MetadataModified 2024-02-10T09:57:35.878771
MetadataPublished
Field Value
Measurement Technique
Measurement Variables