-
Short-RInChIKey=SA-FUHFF-UHFFFADPSC-SHJRUIRDOA-UHFFFADPSC-NUHFF-NUHFF-NUHFF-ZZZ Dataset
To a stirred solution of 1-[(4-tert-butylphenyl)thio]bicyclo[1.1.1]pentane (37.0 mg, 159 μmol, 1.00 equiv.) in methanol (3.00 mL) was added ammonium carbonate (30.6 mg, 318... -
Short-RInChIKey=SA-FUHFF-UHFFFADPSC-IAAVPEBEKX-UHFFFADPSC-NUHFF-NUHFF-NUHFF-ZZZ Dataset
[1.1.1]Propellane (0.6 M in Et2O, 1.00 mL, 600 μmol, 1.00 equiv.) was added to a solution of 3,5-bis(trifluoromethyl)benzenethiol (192 mg, 780 μmol, 1.30 equiv.) in diethyl... -
Short-RInChIKey=SA-FUHFF-UHFFFADPSC-AJKDFBCTGM-UHFFFADPSC-NUHFF-NUHFF-NUHFF-ZZZ Dataset
In a vial, 4-ethoxybenzaldehyde (200 mg, 1.33 mmol, 1.20 equiv) was dissolved in toluene (5.00 mL) and 2-amino-4-chlorobenzenethiol (177 mg, 1.11 mmol, 1.00 equiv) and... -
Short-RInChIKey=SA-FUHFF-UHFFFADPSC-SVTDXKPYBJ-UHFFFADPSC-NUHFF-NUHFF-NUHFF-ZZZ Dataset
In a vial, benzaldehyde (200 mg, 192 μL, 1.89 mmol, 1.20 equiv) was dissolved in toluene (5.00 mL) and 2-amino-4-chlorobenzenethiol (251 mg, 1.57 mmol, 1.00 equiv) and... -
Short-RInChIKey=SA-FUHFF-UHFFFADPSC-XNPQNKNZBZ-UHFFFADPSC-NUHFF-NUHFF-NUHFF-ZZZ Dataset
In a vial, 4-formylbenzonitrile (200 mg, 1.53 mmol, 1.20 equiv) was dissolved in toluene (5.00 mL) and 2-amino-4-chlorobenzenethiol (203 mg, 1.27 mmol, 1.00 equiv) and... -
Short-RInChIKey=SA-FUHFF-UHFFFADPSC-QNPXQKVFKD-UHFFFADPSC-NUHFF-NUHFF-NUHFF-ZZZ Dataset
In a vial, 4-(diethylamino)benzaldehyde (200 mg, 1.1 mmol, 1.20 equiv) was dissolved in toluene (5.00 mL) and 2-amino-4-chlorobenzenethiol (150 mg, 940 μmol, 1.00 equiv) and... -
Short-RInChIKey=SA-FUHFF-UHFFFADPSC-UPRXVIRDQV-UHFFFADPSC-NUHFF-NWMXW-NUHFF-ZZZ Dataset
To a solution of (E)-1-(2-(3,3-diisopropyltriaz-1-en-1-yl)phenyl)cyclopropan-1-amine (152 mg, 582 μmol) in abs. THF, benzoic anhydride (263 mg, 220 μL, 1.16 mmol, 2.00 equiv)... -
Short-RInChIKey=SA-FUHFF-UHFFFADPSC-NJGYPVGPIR-UHFFFADPSC-NUHFF-NUHFF-NUHFF-ZZZ Dataset
The following information was retrieved from the publication:1,2-Addition of Trialkylaluminium Reagents on N-Diphenylphosphinoyl-ketimines in the Absence of Any Additional... -
Short-RInChIKey=SA-FUHFF-UHFFFADPSC-LOXGQIRDJY-UHFFFADPSC-NUHFF-NUHFF-NUHFF-ZZZ Dataset
The following information was retrieved from the publication:1,2-Addition of Trialkylaluminium Reagents on N-Diphenylphosphinoyl-ketimines in the Absence of Any Additional... -
Short-RInChIKey=SA-FUHFF-UHFFFADPSC-NJGYPVGPIR-UHFFFADPSC-NUHFF-NUHFF-NUHFF-ZZZ Dataset
The following information was retrieved from the publication: 1,2-Addition of Trialkylaluminium Reagents on N-Diphenylphosphinoyl-ketimines in the Absence of Any Additional... -
Short-RInChIKey=SA-FUHFF-UHFFFADPSC-MEBOKUYVJS-UHFFFADPSC-NUHFF-NUHFF-NUHFF-ZZZ Dataset
A solution of potassium;hydroxide in water (398 mg, 7.10 mL, 7.10 mmol, 1.00M, 2.01 equiv) was added to a solution of... -
Short-RInChIKey=SA-FUHFF-UHFFFADPSC-ZEQLGGMCOX-UHFFFADPSC-NUHFF-NUHFF-NUHFF-ZZZ Dataset
At 0 °C, potassium;iodide (2.21 g, 13.3 mmol, 0.549 equiv) was added in small portions to a solution of periodic acid (1.00 g, 5.21 mmol, 0.215 equiv) in 80 mL of conc.... -
Short-RInChIKey=SA-FUHFF-UHFFFADPSC-XWTBMUIROL-UHFFFADPSC-NUHFF-NUHFF-NUHFF-ZZZ Dataset
To a solution of 1,1,3,3-tetramethyl-2H-isoindole (4.35 g, 24.8 mmol, 1.00 equiv) in 150 mL of dichloromethane, 3-chlorobenzenecarboperoxoic acid (9.12 g, 37.0 mmol, 1.49... -
Short-RInChIKey=SA-FUHFF-UHFFFADPSC-JXIRPMPWQA-UHFFFADPSC-NUHFF-NUHFF-NUHFF-ZZZ Dataset
The information given below was retrieved and reworked from the publication: Thermal effects in the organocatalytic asymmetric α‑amination of disubstituted aldehydes with... -
Short-RInChIKey=SA-FUHFF-UHFFFADPSC-TYIDFXFGRR-UHFFFADPSC-NUHFF-NUHFF-NUHFF-ZZZ Dataset
The information given below was retrieved and reworked from the publication: Synthesis of Methoxyfumimycin with 1,2-Addition to Ketimines by Patrick J. Gross, Caroline E.... -
Short-RInChIKey=SA-FUHFF-UHFFFADPSC-PEQHIRFAKI-UHFFFADPSC-NUHFF-NUHFF-NUHFF-ZZZ Dataset
In a 500 mL round-bottomed flask, 4-tritylaniline hydrochloride (25.0 g, 67.2 mmol, 1.00 equiv) was suspended in 235 mL of DMF and cooled to –15 °C. At this temperature,... -
Short-RInChIKey=SA-FUHFF-UHFFFADPSC-BIRLDGKMJJ-UHFFFADPSC-NUHFF-NUHFF-NUHFF-ZZZ Dataset
Molecular bromine (19.2 g, 6.16 mL, 120 mmol, 8.00 equiv) was added to a solution of 1,2,2-triphenylethenylbenzene (5.00 g, 15.0 mmol, 1.00 equiv) in 14 mL of glacial acetic... -
Short-RInChIKey=SA-FUHFF-UHFFFADPSC-YBGIIZGNEO-UHFFFADPSC-NUHFF-NUHFF-NUHFF-ZZZ Dataset
Molecular bromine (29.9 g, 9.59 mL, 187 mmol, 12.0 equiv) was added slowly to tritylbenzene (5.00 g, 15.6 mmol, 1.00 equiv) with continuous stirring. The resulting slurry was... -
Short-RInChIKey=SA-FUHFF-UHFFFADPSC-WYNFDKNFCM-UHFFFADPSC-NUHFF-NUHFF-NUHFF-ZZZ Dataset
Under an argon atmosphere, butane;lithium (3.56 g, 22.2 mL, 55.6 mmol, 2.50M, 12.0 equiv) was added drop by drop to a solution of... -
Short-RInChIKey=SA-FUHFF-UHFFFADPSC-ADDOCBLMGW-UHFFFADPSC-NUHFF-NUHFF-NUHFF-ZZZ Dataset
Under an argon atmosphere, butane;lithium (3.56 g, 22.2 mL, 55.6 mmol, 2.50M, 12.0 equiv) was added drop by drop to a solution of...