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Short-RInChIKey=SA-FUHFF-UHFFFADPSC-LYCVEUSFVI-UHFFFADPSC-NUHFF-NLXOS-NUHFF-ZZZ Dataset
(E)-N-(4-bromophenyl)-1-(1H-pyrrol-2-yl)methanimine (151 mg, 606 μmol, 1.20 equiv) was deprotonated using a stoichiometric amount of tBuOK (68.0 mg, 606 μmol, 1.20 equiv) in 5... -
Short-RInChIKey=SA-FUHFF-UHFFFADPSC-XCKQSEIRVZ-UHFFFADPSC-NUHFF-NZOLC-NUHFF-ZZZ Dataset
(E)-1-(1H-Pyrrol-2-yl)-N-(4-(trifluoromethyl)phenyl)methanimine (144 mg, 606 μmol, 1.20 equiv) was deprotonated using a stoichiometric amount of tBuOK (136 mg, 1.21 mmol, 1.20... -
Short-RInChIKey=SA-FUHFF-UHFFFADPSC-QIRBWRVTFH-UHFFFADPSC-NUHFF-NUHFF-NUHFF-ZZZ Dataset
In a vial, 3-azido-1-(2-chloro-4-nitrophenyl)-5-methyl-1H-pyrazole (50.0 mg, 179 μmol, 1.00 equiv) was dissolved in THF (4.00 mL) and water (4.00 mL) (1:1) and copper;sulfate... -
Short-RInChIKey=SA-FUHFF-UHFFFADPSC-UFCSIROIFJ-UHFFFADPSC-NUHFF-NUHFF-NUHFF-ZZZ Dataset
In a vial, 3-azido-5-methyl-1-(4-nitrophenyl)-1H-pyrazole (54.7 mg, 224 μmol, 1.00 equiv) was dissolved in THF (4.00 mL) and water (4.00 mL) (1:1) and copper;sulfate (7.15 mg,... -
Short-RInChIKey=SA-FUHFF-UHFFFADPSC-VTYPYIREEK-UHFFFADPSC-NUHFF-NUHFF-NUHFF-ZZZ Dataset
In a vial, ethyl 3-azido-1-(4-bromobenzyl)-1H-pyrazole-4-carboxylate (50.0 mg, 143 μmol, 1.00 equiv) was dissolved in THF (5.00 mL) and water (5.00 mL) (1:1) and... -
Short-RInChIKey=SA-FUHFF-UHFFFADPSC-YDSBXXBOYI-UHFFFADPSC-NUHFF-NJLCG-NUHFF-ZZZ Dataset
(E)-3-(3,3-Diisopropyltriaz-1-en-1-yl)-1H-pyrazole (500 mg, 2.56 mmol, 1.00 equiv) was dissolved in DMSO (26.0 mL) and cesium carbonate (1.00 g, 3.07 mmol, 1.20 equiv) was... -
Short-RInChIKey=SA-FUHFF-UHFFFADPSC-FZCYRDQIRB-UHFFFADPSC-NUHFF-LUHFF-NUHFF-ZZZ Dataset
Diphenyl(2-pyridinyl)phosphine (1.84 g, 7.00 mmol, 3.00 eq.), CuCl (0.231 g, 2.33 mmol, 1.00 eq.) and AgCl (0.334 g, 2.33 mmol, 1.00 eq.) were suspended in 15 mL of... -
Short-RInChIKey=SA-FUHFF-UHFFFADPSC-TZKIRFQAWQ-UHFFFADPSC-NUHFF-LUHFF-NUHFF-ZZZ Dataset
Diphenyl(2-pyridyl)phosphine (1.0 g, 3.80 mmol, 3.00 equiv), CuI (241 mg, 1.26 mmol, 1.00 equiv) and AgI (297 mg, 1.26 mmol, 1.00 equiv) were suspended in 15 mL of... -
Short-RInChIKey=SA-FUHFF-UHFFFADPSC-RRQCZUMLBW-UHFFFADPSC-NUHFF-NGNNP-NUHFF-ZZZ Dataset
The information given below was retrieved and reworked from the publication: Microwave-Assisted Stereoselective One-Pot Synthesis of Symmetrical and Unsymmetrical... -
Short-RInChIKey=SA-FUHFF-UHFFFADPSC-GIIRFSVKDF-UHFFFADPSC-NUHFF-NUHFF-NUHFF-ZZZ Dataset
9-(4-Bromophenyl)-3,6-dimethoxycarbazole (1.00 g, 2.62 mmol, 1.00 equiv), 4,4,5,5-tetramethyl-2-thiophen-2-yl-1,3,2-dioxaborolane (605 mg, 2.88 mmol, 1.10 equiv), Pd(dppf)Cl2... -
Short-RInChIKey=SA-FUHFF-UHFFFADPSC-OYFFSPILVQ-UHFFFADPSC-NUHFF-NUHFF-NUHFF-ZZZ Dataset
9H-Carbazole (500 mg, 2.99 mmol, 1.00 equiv) and zinc dichloride (856 mg, 6.28 mmol, 2.10 equiv) were dried in a vial. Nitromethane (10 mL) was added under argon atmosphere. A... -
Short-RInChIKey=SA-FUHFF-UHFFFADPSC-VIRDEPYHHG-UHFFFADPSC-NUHFF-MUHFF-NUHFF-ZZZ Dataset
Methyl 3-(1-bicyclo[1.1.1]pentanylsulfonyl)propanoate (1.36 g, 6.22 mmol, 1.00 equiv) was dissolved in tetrahydrofuran (14 mL) and stirred at 21 °C. Potassium tert-butoxide in... -
Short-RInChIKey=SA-FUHFF-UHFFFADPSC-UAOMNDAJRK-UHFFFADPSC-NUHFF-NUHFF-NUHFF-ZZZ Dataset
4-Bromonaphthalen-2-ol (6.25 g, 28.0 mmol, 1.00 equiv) was dissolved in dichloromethane (150 mL) and chlorocopper(1+);2-(dimethylamino)ethyl-dimethyl-amine (32.5 mg, 140 μmol,... -
Short-RInChIKey=SA-FUHFF-UHFFFADPSC-YBGIIZGNEO-UHFFFADPSC-NUHFF-NUHFF-NUHFF-ZZZ Dataset
Molecular bromine (29.9 g, 9.59 mL, 187 mmol, 12.0 equiv) was added slowly to tetraphenylmethane (5.00 g, 15.6 mmol, 1.00 equiv) with continous stirring. The resulting slurry... -
Short-RInChIKey=SA-FUHFF-UHFFFADPSC-PEQHIRFAKI-UHFFFADPSC-NUHFF-NUHFF-NUHFF-ZZZ Dataset
In a 500 mL round bottom flask,4-tritylaniline hydrochloride (23.2 g, 62.3 mmol, 1.00 equiv) was suspended in 235 mL of N,N-dimethylformamide and cooled to -15 °C. At this... -
Short-RInChIKey=SA-FUHFF-UHFFFADPSC-SXBGVJQQQN-UHFFFADPSC-NUHFF-NUHFF-NUHFF-ZZZ Dataset
In a three-necked round bottom flask to a stirred solution of methyl 2-hydroxy-4-(trifluoromethyl)benzoate (2.50 g, 11.36 mmol, 1.00 equiv) in DCM (10.0 mL) under inert... -
Short-RInChIKey=SA-FUHFF-UHFFFADPSC-IRELIHAAUC-UHFFFADPSC-NUHFF-NUHFF-NUHFF-ZZZ Dataset
In a round bottom flask to a stirred solution of 2-hydroxy-4-(trifluoromethyl)benzoic acid (3.00 g, 14.55 mmol, 1.00 equiv) in methanol (15.0 mL) was added concentrated... -
Short-RInChIKey=SA-FUHFF-UHFFFADPSC-NGRMNRCBYX-UHFFFADPSC-NUHFF-NUHFF-NUHFF-ZZZ Dataset
To a solution of 4,16-dibromo[2,2]paracyclophane (2.90 g, 7.92 mmol, 1.00 equiv.) in toluene (100.0 mL) was added benzophenone imine (1.51 g, 8.32 mmol, 1.05 equiv.),... -
Short-RInChIKey=SA-FUHFF-UHFFFADPSC-GAUNOMJAIR-UHFFFADPSC-NUHFF-NUHFF-NUHFF-ZZZ Dataset
2-Pyridinamine (600 mg, 6.38 mmol, 1.00 equiv) and 2-bromo-4,5-dimethoxybenzaldehyde (1.56 g, 6.38 mmol, 1.00 equiv) were dissolved in methanol (10 mL).... -
Short-RInChIKey=SA-FUHFF-UHFFFADPSC-GAUNOMJAIR-UHFFFADPSC-NUHFF-NUHFF-NUHFF-ZZZ Dataset
2-Pyridinamine (600 mg, 6.38 mmol, 1.00 equiv) and 2-bromo-4,5-dimethoxybenzaldehyde (1.56 g, 6.38 mmol, 1.00 equiv) were dissolved in methanol (10 mL)....
