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Short-RInChIKey=SA-FUHFF-UHFFFADPSC-OGCOPTUVYR-UHFFFADPSC-NUHFF-NUHFF-NUHFF-ZZZ Dataset
To a solution of 3,6-diphenyl-9H-carbazole (100 mg, 313 μmol, 1.00 equiv) in acetic acid (10 mL) was added molecular bromine (210 mg, 67.8 μL, 1.31 mmol, 4.20 equiv). The... -
Short-RInChIKey=SA-FUHFF-UHFFFADPSC-HEIIGJFYWA-UHFFFADPSC-NUHFF-NUHFF-NUHFF-ZZZ Dataset
Ethyl (E)-2-(4-cyano-3-(3,3-diisopropyltriaz-1-en-1-yl)-1H-pyrazol-1-yl)acetate (428 mg, 1.40 mmol, 1.00 equiv) was dissolved in methylene chloride (30.0 mL). The solution was... -
Short-RInChIKey=SA-FUHFF-UHFFFADPSC-YDUVZTACEK-UHFFFADPSC-NUHFF-NUHFF-NUHFF-ZZZ Dataset
The information given below was retrieved and reworked from the publication: Porous Polymer Networks: Synthesis, Porosity, and Applications in Gas Storage/Separation by... -
Short-RInChIKey=SA-FUHFF-UHFFFADPSC-RUGUWNHIXP-UHFFFADPSC-NUHFF-LUHFF-NUHFF-ZZZ Dataset
For crystallisation of the complex, the ligand C23H38N8 (23.5 mg, 55.0 μmol, 1.10 equiv) and dichlorocopper (6.72 mg, 50.0 μmol, 1.00 equiv) were diluted in MeCN (1 mL). The... -
Short-RInChIKey=SA-FUHFF-UHFFFADPSC-GGYQDMHUVM-UHFFFADPSC-NUHFF-NUHFF-NUHFF-ZZZ Dataset
In a 500 mL round bottom flask with a reflux condenser, trityl chloride (25.0 g, 89.7 mmol, 1.00 equiv.) and aniline (21.7 g, 21.3 mL, 233 mmol, 2.60 equiv.) were stirred for... -
Short-RInChIKey=SA-FUHFF-UHFFFADPSC-PJLMQMBEXP-UHFFFADPSC-NUHFF-NUHFF-NUHFF-ZZZ Dataset
The experiment was carried out using Schlenk technique with nitrogen (99.996%, dried over phosphorus pentoxide) as inert gas. 2-Aminobenzylamine (13.90 g, 113.8 mmol, 1 eq.)... -
Short-RInChIKey=SA-FUHFF-UHFFFADPSC-ARVDXDODRG-UHFFFADPSC-NUHFF-NXYUF-NUHFF-ZZZ Dataset
To an ice-cold and stirred solution of ethyl cis-2-amino-1-cyclohexanecarboxylate hydrochloride (3.00 g, 14.40 mmol, 1.0 eq.) and Et3N (4.20 ml, 30.30 mmol, 2.1 eq) in MeCN... -
Short-RInChIKey=SA-FUHFF-UHFFFADPSC-AQTVUYPMQT-UHFFFADPSC-NUHFF-NUHFF-NUHFF-ZZZ Dataset
[2.2]Paracyclophane (4.0 g, 19.2 mmol, 1.00 equiv.) was dissolved in dichloromethane (380 mL) and cooled to 0 °C. A mixture of sulfuric acid (95% aq. solution, 4.31 mL, 76.8... -
Short-RInChIKey=SA-FUHFF-UHFFFADPSC-GJUZUVZHQF-UHFFFADPSC-NUHFF-NUHFF-NUHFF-ZZZ Dataset
To a solution of 2,4,6-tris(4-bromophenyl)-1,3,5-triazine (1.00 g, 1.83 mmol, 1.00 equiv) in 150 mL of dry THF, butane;lithium (504 mg, 3.15 mL, 7.88 mmol, 2.50M, 4.30 equiv)... -
Short-RInChIKey=SA-FUHFF-UHFFFADPSC-SXPUVBFQXJ-UHFFFADPSC-NUHFF-NUHFF-NUHFF-ZZZ Dataset
1,2-Bis(2-furyl)-2-hydroxy-ethanone (400 mg, 2.08 mmol, 1.00 equiv) and pyridiniumchlorochromate (673 mg, 3.12 mmol, 1.50 equiv) were suspended in dichloromethane (15.0 mL)... -
Short-RInChIKey=SA-FUHFF-UHFFFADPSC-YBGSMMQIEM-UHFFFADPSC-NUHFF-NOCXD-NUHFF-ZZZ Dataset
N-Benzylideneaniline (906 mg, 5.00 mmol, 1.00 equiv) and sodium;cyanide (49.0 mg, 1.00 mmol, 0.200 equiv) was evacuated in a schlenk tube. N,N-dimethylformamide (30.0 mL) was... -
Short-RInChIKey=SA-FUHFF-UHFFFADPSC-SGRXMHUVMD-UHFFFADPSC-NUHFF-NUHFF-NUHFF-ZZZ Dataset
The starting material (48.5 mg, 204 μmol, 1.00 equiv) was dissolved under inert atmosphere in 3 mL of dry DMF. Sodium hydride (8.99 mg, 225 μmol, 1.10 equiv) and 1-iodobutane... -
Short-RInChIKey=SA-FUHFF-UHFFFADPSC-UMLFTCYAQP-UHFFFADPSC-NUHFF-NUHFF-NUHFF-ZZZ Dataset
To a stirred solution of p-tolunitrile (10.0 g, 85 mmol, 1.00 equiv) in 100 mL of CHCl3 was added NBS (15.6 g, 88 mmol, 1.03 equiv) and benzoyl peroxide (2.07 g, 8.5 mmol,... -
Short-RInChIKey=SA-FUHFF-UHFFFADPSC-LVGOHACWPD-UHFFFADPSC-NUHFF-NUVBP-NUHFF-ZZZ Dataset
Under an Ar atmosphere, 95 mg of the porphyrin (124 µmol, 1.00 equiv.), 265 mg of 3,4,5-(trifluorophenyl)boronic acid (1.51 mmol, 12.2 equiv.), 650 mg of K3PO4 (3.06 mmol,... -
Short-RInChIKey=SA-FUHFF-UHFFFADPSC-GCSKMOXHRG-UHFFFADPSC-NUHFF-NUHFF-NUHFF-ZZZ Dataset
To a solution of (4-(2-bromo-3-((5-iodobenzo[d][1,3]dioxol-4-yl)methoxy)-4-methoxyphenyl)-4-((tert-butyldimethylsilyl)oxy)but-2-yn-1-yl)trimethylsilane (115 mg, 191 μmol, 1.00... -
Short-RInChIKey=SA-FUHFF-UHFFFADPSC-LNZKUVPJCK-UHFFFADPSC-NUHFF-NUHFF-NUHFF-ZZZ Dataset
In a vial fitted with a magnetic stirring bar, potassium 4-trifluoroborate[2.2]paracyclophane (188.5 mg, 0.06 mmol, 1.50 equiv.), potassium phosphate (339.6 mg, 1.60 mmol,... -
Short-RInChIKey=SA-FUHFF-UHFFFADPSC-RJOYWTPJYZ-UHFFFADPSC-NUHFF-NUHFF-NUHFF-ZZZ Dataset
Bromine (3.92 g, 1.26 mL, 25.0 mmol, 1.00 equiv.) was diluted with dichloromethane (40 mL). From this solution, 5.0 mL were added to iron powder (27.0 mg, 483 μmol, 2.0 mol%)... -
Short-RInChIKey=SA-FUHFF-UHFFFADPSC-NFZAQQZYIY-UHFFFADPSC-NUHFF-NUHFF-NUHFF-ZZZ Dataset
S-phenyl-S-bicyclo[1.1.1]pentylsulfoximine (50 mg, 241 µmol, 1.00 equiv.), Cu2O (6.9 mg, 48.2 µmol, 20 mol%) and KOtBu (54 mg, 482 µmol, 2.00 equiv.) were mixed in a dry vial... -
Short-RInChIKey=SA-FUHFF-UHFFFADPSC-YUVGKANYCT-UHFFFADPSC-NUHFF-NUHFF-NUHFF-ZZZ Dataset
To a vial (5.0 mL) containing a stirring bar, tris(4-iodophenyl)amine (99.7 mg, 160 μmol, 1.00 equiv), potassium tert-butoxide (162 mg, 1.44 mmol, 9.00 equiv) and... -
Short-RInChIKey=SA-FUHFF-UHFFFADPSC-YUVPQEFJXV-UHFFFADPSC-NUHFF-NUHFF-NUHFF-ZZZ Dataset
The following information was retrieved from the publication:1,2-Addition of Trialkylaluminium Reagents on N-Diphenylphosphinoyl-ketimines in the Absence of Any Additional...
